This file contains only basic metadata and links to where the website can be accessed. As a result, the licence under which this file is shared on OpenAIR is not necessarily the same as the licence used for the website content itself. Please consult the terms and conditions of use for the website directly. GENERAL INFORMATION 1. Title of website: Neutron diffraction assessment at extreme temperatures to gain insights into the performance of thermocouple coatings. Part 1. [Dataset] 2. Contributor information: Irungu, Beth Faisal, Nadimul (Robert Gordon University) Lee, Tung Lik Goel, Saurav Ismail, Mubarak Abdelrasoul Elnour 3. Date on which website first launched: 2025-03-14 ACCESS INFORMATION 1. Release Date and Access Link: This file is due to be publicly released on the 15th March 2028. Full metadata is available from the ISIS neutron and muon source data journal: https://doi.org/10.5286/ISIS.E.RB2510004-1 2. Recommended citation: IRUNGU, B., FAISAL, N., LEE, T.L., GOEL, S. and ISMAIL, M.A.E. 2025. Neutron diffraction assessment at extreme temperatures to gain insights into the performance of thermocouple coatings. Part 1. [Dataset]. Hosted on STFC ISIS neutron and muon source data journal [online]. Available from: https://doi.org/10.5286/ISIS.E.RB2510004-1 CONTEXTUAL INFORMATION 1. Abstract: This project investigates the behaviour of Chromel-Alumel K-type thermocouples under extreme temperature conditions, focusing on coatings produced through thermal spray processes. These thermocouples, widely used in industrial and aerospace applications, experience phase changes that can compromise temperature accuracy, particularly in cryogenic environments. While bulk material behaviour is well-documented, the performance of thin films and coatings remains poorly understood, especially under high and low temperatures. The proposed study employs neutron diffraction to assess in-situ phase transformations and residual stress effects in Ni-20Cr coatings. Neutron diffraction's deep material penetration and high resolution make it ideal for probing changes across coating thicknesses. The project will investigate the influence of residual stress on phase transformations, contributing to improved thermocouple calibration and performance in cryogenic and high-temperature applications. By addressing these material challenges, the research aligns with ongoing UK government initiatives to digitalize manufacturing processes, building on previous EPSRC-funded projects and supporting the completion of a PhD thesis on thermal spray coatings with embedded sensing capabilities.